One-pot Microwave-Assisted Synthesis of 1H-Phenanthro[9,10- d][1,2,3]triazole

Abstract

In this study, a fast and good yield one-pot microwave-assisted synthesis (45 seconds) of 1H-phenanthro[9,10-d][1,2,3]triazole by a 1,3-dipolar cycloaddition reaction of sodium azide and 9-bromophenanthrene in the presence of potassium tert-butoxide in DMSO as solvent is reported.

Keywords

• Microwave assisted synthesis
• 1
• 3-Dipolar cycloadditions
• Benzyne intermediate
• 1H-Phenanthro[9
• 10-d][1
• 2
• 3]triazole
• 1
• 2
• 3-Triazoles