Crystals (Sep 2022)

Reaction-Time-Dependent Opto-Electrical Properties of Graphene Oxide

  • Muhammad Kashif,
  • Norah Salem Alsaiari,
  • Erdawaty Jaafar,
  • Foo Wah Low,
  • Cheen Sean Oon,
  • Siti Kudnei Sahari,
  • Nayef S. Almuaikel

DOI
https://doi.org/10.3390/cryst12091303
Journal volume & issue
Vol. 12, no. 9
p. 1303

Abstract

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The reaction-time-dependent synthesis of graphene oxide (GO) was carried out using a modified Hummer’s method. The drop-casting method was used to coat GO films on a glass substrate. Various techniques, including scanning electron microscopy, X-ray diffraction, UV–Vis spectroscopy (UV–Vis), Fourier transform infrared spectroscopy, and current–voltage characteristics, were performed to obtain the morphological, structural, optical, and electrical properties of GO. Morphological structural observations revealed that more oxygen functional groups were present as the reaction time increased from 24 to 96 h, which was confirmed by the optical properties of GO thin films. The resistivity of the as-deposited films increased from 9.74 × 106 to 26.85 × 106 Ω·cm as the reaction time increased. The optimized reaction time with a resistivity of 12.13 × 106 Ω·cm was 48 h, as demonstrated by morphological and optical data.

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