IUCrData
(Feb 2017)
2,5-Bis[(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl)sulfanyl]-1,3,4-thiadiazole
Gabriel Partl,
Gerhard Laus,
Klaus Wurst,
Holger Kopacka,
Thomas Müller,
Hubert Huppertz,
Herwig Schottenberger
Affiliations
Gabriel Partl
University of Innsbruck, Faculty of Chemistry and Pharmacy, Innrain 80, 6020 Innsbruck, Austria
Gerhard Laus
University of Innsbruck, Faculty of Chemistry and Pharmacy, Innrain 80, 6020 Innsbruck, Austria
Klaus Wurst
University of Innsbruck, Faculty of Chemistry and Pharmacy, Innrain 80, 6020 Innsbruck, Austria
Holger Kopacka
University of Innsbruck, Faculty of Chemistry and Pharmacy, Innrain 80, 6020 Innsbruck, Austria
Thomas Müller
University of Innsbruck, Faculty of Chemistry and Pharmacy, Innrain 80, 6020 Innsbruck, Austria
Hubert Huppertz
University of Innsbruck, Faculty of Chemistry and Pharmacy, Innrain 80, 6020 Innsbruck, Austria
Herwig Schottenberger
University of Innsbruck, Faculty of Chemistry and Pharmacy, Innrain 80, 6020 Innsbruck, Austria
DOI
https://doi.org/10.1107/S2414314617001109
Journal volume & issue
Vol. 2,
no. 2
p.
x170110
Abstract
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The title compound, C18H8F26N2S3, was obtained by double S-perfluorohexylethylation of dipotassium 1,3,4-thiadiazole-2,5-dithiolate in methanol. The molecule exhibits twofold rotational symmetry, with the S atom lying on the rotation axis. The fluorocarbon chains adopt helical conformations and the F atoms of the two terminal C atoms are disordered over two sets of sites. No directional intermolecular interactions occur in the crystal.
Keywords
Published in IUCrData
ISSN
2414-3146 (Online)
Publisher
International Union of Crystallography
Country of publisher
United Kingdom
LCC subjects
Science: Chemistry: Crystallography
Website
https://iucrdata.iucr.org
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