FUNCTIONALIZATION OF TEXTILE FABRICS WITH MICROENCAPSULATED VITAMIN E

Abstract

In this study the experimental deposition of vitamin E microcapsules by padding technique on the textile support made of 50% cotton and 50% polyamide high tenacity Nm 50/1 were performed. The preliminary preparation of textile materials has been made in four consecutive sequences: hot alkaline treatment in absence of NaOH, bleaching, drying and curing. In the pretreatment of textile materials the crosslinking agent Itobinder AG is used, which is an anionic emulsion based on the acrylic copolimer, being followed by the application of a dispersion with content of vitamin E microcapsules. In the present raport the evaluation of obtained performances was made through SEM, GC and FTIR-ATR analysis. By SEM has been determined the wash durability of deposition of vitamin E microcapsules before and after one washing cycle. Following qualitative analysis by Gas-Chromatography coupled with Mass Spectrometry and Fourier Transform Infrared Spectroscopy with Attenuated Total Reflection absorption the related compoundes presents on the surface of the textile materials were identified. After retention time the vitamin E acetate is found with preponderance in all chromatograms at 15, 70 min with aproximation. Also by FTIR-ATR the presence of vitamin E acetate is confirmed by the apparition of a new peak at 1731 cm-1 and changes of intensity of various peaks, especially in the fingerprint region of the spectra of the functionalized fabrics.

Keywords

• textiles
• microcapsules
• vitamin Eacetate
• FTIR-ATR
• SEM
• GC-MS