Spectral Analysis and Structural Elucidation of Luliconazole

LIN Yun-liang; GAO Hong-mei; LI Feng; CHEN Xiang-feng

doi:10.11938/cjmr20182620

Chinese Journal of Magnetic Resonance (Sep 2018)

Spectral Analysis and Structural Elucidation of Luliconazole

LIN Yun-liang,
GAO Hong-mei,
LI Feng,
CHEN Xiang-feng

Affiliations

LIN Yun-liang: Shandong Analysis and Test Center, Qilu University of Technology(Shandong Academy of Sciences), Ji'nan 250014, China
GAO Hong-mei: Shandong Analysis and Test Center, Qilu University of Technology(Shandong Academy of Sciences), Ji'nan 250014, China
LI Feng: Shandong Analysis and Test Center, Qilu University of Technology(Shandong Academy of Sciences), Ji'nan 250014, China
CHEN Xiang-feng: Shandong Analysis and Test Center, Qilu University of Technology(Shandong Academy of Sciences), Ji'nan 250014, China

DOI: https://doi.org/10.11938/cjmr20182620
Journal volume & issue: Vol. 35, no. 3
pp. 385 – 392

Abstract

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Infrared spectra, ultraviolet spectra, nuclear magnetic resonance (NMR) spectra (i.e., 1H NMR, 13C NMR, DEPT135, 1H-1H COSY, 1H-13C HMQC and 1H-13C HMBC) and mass spectra of luliconazole were collected and used to characterize the compound. Differential scanning calorimetry, X-ray power diffraction and elementary analysis were also performed. All 1H and 13C NMR signals of the compound were assigned. The structure of the compound was determined.

Published in Chinese Journal of Magnetic Resonance

ISSN: 1000-4556 (Print)
Publisher: Science Press
Country of publisher: China
LCC subjects: Science: Physics: Electricity and magnetism
Website: http://121.43.60.238/bpxzz/EN/1000-4556/home.shtml

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