Dimethyl 2-nitrobiphenyl-4,4′-dicarboxylate

Vanessa C. M. Vieira; James A. Golen; Arnold L. Rheingold; David R. Manke

doi:10.1107/s1600536814004218

Acta Crystallographica Section E (Mar 2014)

Dimethyl 2-nitrobiphenyl-4,4′-dicarboxylate

Vanessa C. M. Vieira,
James A. Golen,
Arnold L. Rheingold,
David R. Manke

Affiliations

Vanessa C. M. Vieira: Department of Chemistry and Biochemistry, University of Massachusetts Dartmouth, 285 Old Westport Road, North Dartmouth, MA 02747, USA
James A. Golen: Department of Chemistry, University of California, San Diego, 9500 Gilman Drive, La Jolla, CA 92093, USA
Arnold L. Rheingold: Department of Chemistry, University of California, San Diego, 9500 Gilman Drive, La Jolla, CA 92093, USA
David R. Manke: Department of Chemistry and Biochemistry, University of Massachusetts Dartmouth, 285 Old Westport Road, North Dartmouth, MA 02747, USA

DOI: https://doi.org/10.1107/s1600536814004218
Journal volume & issue: Vol. 70, no. 3
pp. o371 – o371

Abstract

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The title compound, C16H13NO6, exhibits a biphenyl unit with a dihedral angle between the two aryl rings of 56.01 (5)°. The two ester groups vary slightly from planarity, with aryl–ester dihedral angles of 4.57 (5) and 16.73 (5)°. The nitro group is turned from the aromatic unit with an aryl–nitro dihedral angle of 48.66 (4)°. In the crystal, molecules are connected by weak C—H...O interactions, forming a three-dimensional network.

Published in Acta Crystallographica Section E

ISSN: 1600-5368 (Online)
Publisher: International Union of Crystallography
Country of publisher: United Kingdom
LCC subjects: Science: Chemistry: Crystallography
Website: https://journals.iucr.org/e/

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