Journal of Synchrotron Radiation (Jan 2024)

Improvement of ultra-small-angle XPCS with the Extremely Brilliant Source

  • William Chèvremont,
  • Thomas Zinn,
  • Theyencheri Narayanan

DOI
https://doi.org/10.1107/S1600577523008627
Journal volume & issue
Vol. 31, no. 1
pp. 65 – 76

Abstract

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Recent technical developments and the performance of the X-ray photon correlation spectroscopy (XPCS) method over the ultra-small-angle range with the Extremely Brilliant Source (EBS) at the ESRF are described. With higher monochromatic coherent photon flux (∼1012 photons s−1) provided by the EBS and the availability of a fast pixel array detector (EIGER 500K detector operating at 23000 frames s−1), XPCS has become more competitive for probing faster dynamics in relatively dilute suspensions. One of the goals of the present development is to increase the user-friendliness of the method. This is achieved by means of a Python-based graphical user interface that enables online visualization and analysis of the processed data. The improved performance of XPCS on the Time-Resolved Ultra-Small-Angle X-ray Scattering instrument (ID02 beamline) is demonstrated using dilute model colloidal suspensions in several different applications.

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