Novos sorventes baseados em poli (metiloctilsiloxano) sobre sílica para uso em extração em fase sólida New sorbents based on poly(methyloctylsiloxane) immobilized on silica for use in solid-phase extraction

Abstract

This paper presents an easy and practical procedure to obtain silica-based C-8 type sorbents for use in solid-phase extraction. The materials are prepared by depositing poly(methyloctylsiloxane), PMOS, on the silica support. Two different treatments for immobilization were used: thermal treatment or gamma irradiation. Suitable recoveries were obtained after pre-concentration of dilute solutions, at the ng/L level, of a mixture of pesticides, indicating the good performance of the materials.

Keywords

• pesticides
• solid-phase extraction
• sorbents