Molbank (Nov 2012)

3,5-Bis(4-dodecylthiophen-2-yl)-4H-1,2,6-thiadiazin-4-one

  • Panayiotis A. Koutentis,
  • Heraklidia A. Ioannidou

DOI
https://doi.org/10.3390/M784
Journal volume & issue
Vol. 2012, no. 4
p. M784

Abstract

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3,5-Dichloro-4H-1,2,6-thiadiazin-4-one 1 reacts with (4-dodecylthiophen-2-yl)trimethylstannane 4 (2.2 equiv.) and Pd(Ph3P)2Cl2 (5 mol%) in acetonitrile at ca. 82 °C to give 3,5-bis(4-dodecylthiophen-2-yl)-4H-1,2,6-thiadiazin-4-one 5 in 93% yield.

Keywords