Particle Sizing and Surface Area Measurements: A Comparative Assessment of Commercial Air Permeability and Laser Light Diffraction Instruments

Abstract

Six different commercial powders, finer than 45 μm, were used for examining the effects of particle characteristics on mean particle size and specific surface area. The measurements were carried out using the most commonly used air permeability- and laser light diffraction (scattering) techniques. As the air permeability method has been used as a benchmark for decades in the powder metallurgy (P/M) industry, the physical phenomena that govern the passage of gas through the powder bed under laminar flow conditions were also presented. The experimental data indicate that both methods give similar results for spherical powders. The advantage of laser light systems over gas permeameters is the ability to provide additional information on particle size distribution. Irregularly shaped powders should be analyzed by both techniques, relying on gas permeametry for surface area measurements and on laser light diffraction for the estimation of mean particle size and size distribution. Application of scanning electron microscopy as a complementary technique was found very helpful in the interpretation of data through visualization of individual particles.

Keywords

• gas permeametry
• Kozeny–Carman equation
• specific surface area
• laser light scattering
• particle size analysis