Tecnologia em Metalurgia, Materiais e Mineração (Jun 2014)

USE OF-EPR-DL FIELD TEST EQUIPMENT FOR DETECTION OF SIGMA PHASE

  • Abraão Danilo Gomes Barreto,
  • Tathiane Caminha Andrade,
  • Cleiton Carvalho Silva,
  • Hélio Cordeiro de Miranda

DOI
https://doi.org/10.4322/tmm.2014.022
Journal volume & issue
Vol. 11, no. 2
pp. 146 – 154

Abstract

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This work has objective to correlate the intergranular corrosion susceptibility test named EPR-DL (Electrochemical Potentiokinetic Reactivation of Double Loop) with the sigma phase formation and other phases. It has been used samples from a UNS S32760 steel pipe for conducting various aging heat treatments. Held isothermal heat treatment at 850°C for 1 min, 10 min, 30 min, 1 h, 1h30min and 10 h. Each heat treated sample and as received were tested using the electrochemical polarization reactivation of double loop technique (EPR-DL). It was possible the detection of deleterious phases with DL-EPR portable cell. The EPR-DL test of some samples showed a second peak of reactivation in which the results showed that this peak might be associated with ferrite or be related to the presence of chi phase

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