Journal of Synchrotron Radiation (Mar 2025)

New online beam intensity synchronous monitoring system in scanning transmission X-ray microscopy

  • Yuchen Jiao,
  • Xiangzhi Zhang,
  • Zijian Xu,
  • Zhen Yao,
  • Tianxiao Sun,
  • Yufei Zhang,
  • Bo Zhao,
  • Zhi Guo,
  • Yong Wang,
  • Xiangjun Zhen,
  • Haigang Liu,
  • Shasha Liang,
  • Haitao Li,
  • Xuanyu Zhao,
  • Jian He,
  • Renzhong Tai

DOI
https://doi.org/10.1107/s1600577524012141
Journal volume & issue
Vol. 32, no. 2
pp. 424 – 431

Abstract

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The scanning transmission X-ray microscopy (STXM) platform based on synchrotron radiation has achieved nanoscale imaging with chemical sensitivity using spectro-microscopy techniques. However, the quality of STXM imaging is affected by the stability of the beam intensity. The top-up operation mode of synchrotrons to maintain a constant electron beam intensity introduces periodic fluctuations in the X-ray beam intensity, leading to notable imaging noise that decreases both contrast and precision. To address this issue, a high-speed real-time beam intensity monitoring system was designed and implemented at the BL08U1A beamline of the Shanghai Synchrotron Radiation Facility. This system utilizes an yttrium–aluminium–garnet crystal along with dual detectors having an acquisition frequency of up to 1 MHz and a synchronization error of less than 20 ns between them. This system can precisely and synchronously monitor the X-ray beam intensity variations which are used to remove noise due to electron injection from STXM images, thereby markedly improving the quality of STXM imaging.

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