Acta Crystallographica Section E (Apr 2013)

2-(2-Chlorophenyl)-N-cyclohexyl-2-oxoacetamide

  • Xiu-Dan Jin,
  • Jin-Long Wu

DOI
https://doi.org/10.1107/S1600536813005904
Journal volume & issue
Vol. 69, no. 4
pp. o505 – o505

Abstract

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In the title compound, C14H16ClNO2, the cyclohexyl ring has a chair conformation. The dihedral angle between the benzene ring and the mean plane of the four planar C atoms of the cyclohexyl ring is 45.2 (3)°. The two carbonyl groups are trans to one another, with an O=C—C=O torsion angle of −137.1 (3)°. In the crystal, molecules are linked by N—H...O hydrogen bonds forming chains propagating along [001]. A region of disordered electron density, situated near the unit-cell corners, was treated using the SQUEEZE routine in PLATON [Spek (2009). Acta Cryst. D65, 148–155]. It gave a solvent-accessible void of ca 400 Å3 for only 21 electrons. It is probably due to traces of the solvent of crystallization and was not taken into account during structure refinement.