Effect of Cold Rolling on Cluster(1) Dissolvability during Artificial Aging and Formability during Natural Aging in Al-0.6Mg-1.0Si-0.5Cu Alloy

Abstract

Natural aging after solution treatment has a negative effect on the precipitation strengthening of Al–Mg–Si alloys since Cluster(1) formed at a room temperature cannot be dissolved or transformed into precipitates during artificial aging at 170 °C. In this study, cold rolling is focused on as an alternative solution to pre-aging, which is a conventional method to prevent Cluster(1) formation. It is known that excess vacancies are necessary for cluster formation. Cold rolling suppresses cluster formation because excess vacancies disappear at dislocations introduced by cold rolling. In addition, it is expected that cold rolling accelerates the precipitation behavior because the diffusion of solute atoms is promoted by introduced lattice defects. The transition of Cluster(1) was evaluated by Micro Vickers hardness tests, tensile tests, electrical conductivity measurements and differential scanning calorimetry analyses. Results showed the negative effect of natural aging was almost suppressed in 10% cold-rolled samples and completely suppressed in 30% cold-rolled samples since Cluster(1) dissolved during artificial aging at 170 °C due to lowering of the temperature of Cluster(1) dissolution by cold rolling. It was found that the precipitation in cold-rolled samples was accelerated since the hardness peak of 10% cold-rolled samples appeared earlier than T6 and pre-aged samples.

Keywords

• Al–Mg–Si alloy
• natural aging
• cold rolling
• differential scanning calorimetry