Materials Research (May 2021)

Influence of Plasma Nitriding with a Nitrogen Rich Gas Composition on the Reciprocating Sliding Wear of a DIN 18MnCrSiMo6-4 Steel

  • Rafael Luciano Dalcin,
  • Alexandre da Silva Rocha,
  • Victor Velho de Castro,
  • Leonardo Fonseca Oliveira,
  • Julio Cesar Klein das Neves,
  • Carlos Henrique da Silva,
  • Célia de Fraga Malfatti

DOI
https://doi.org/10.1590/1980-5373-mr-2020-0592
Journal volume & issue
Vol. 24, no. 4

Abstract

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In this study, the sliding wear of a DIN 18MnCrSiMo6-4 continuous cooling bainitic steel plasma nitrided with a nitrogen rich gas composition was investigated. To evaluate the influence of processing time and temperature on mechanical and microstructural characteristics of nitrided layer, the samples were nitrided at 400, 450, 500 and 550 °C for 3, 6 and 9 h. The produced nitrided layers were characterized concerning the microstructure, phase composition, microhardness and surface roughness. The samples were tested by ball-on-flat reciprocating dry sliding for friction coefficient and wear analysis. The tests were stopped after a given damage criteria involving the rapid growth of the friction coefficients and wear. The correlation of the different treatment parameters and resulting case depths and surface hardness with sliding distance at the time of microcracks formation or delamination of the surface layer was evaluated statistically by the analysis of variance (ANOVA). The plasma nitrided samples at 550 °C showed better wear performances in the ball-on-flat tests than the other groups investigated, since these samples have a thicker compound layer and diffusion zone higher than the other conditions investigated. In general, the beginning wear is slower because of the hardest region of the compound layer.

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