Investigation of Microstructural, Mechanical, and Tribological Properties of TiC and MWCNT Reinforced Hot-Pressed Scalmalloy^® Hybrid Composites

Abstract

In this study, hybrid composite materials were fabricated using a Scalmalloy® matrix with fixed multi-walled carbon nanotube (MWCNT, 0.8%) content and varying titanium carbide (TiC; 5%, 10%, 15%) reinforcements via the hot-pressing method. Unlike conventional approaches in the literature that utilize additive manufacturing, this research presents the first successful production of Scalmalloy®-based hybrid composites through a traditional powder metallurgy method. This method enabled the development of a more homogeneous and equiaxed microstructure. The composites were characterized using SEM, EDS, MAP, and XRD analyses, along with density and microhardness measurements. Mechanical performance was evaluated through Vickers hardness and transverse rupture strength (TRS) tests, while dry sliding wear behavior was examined in detail. The hardness of the 15% TiC + 0.8% MWCNT-reinforced composite increased from 87 HV to 181 HV (a 108% improvement), and TRS increased from 354 MPa to 545 MPa (a 54% improvement). Additionally, wear surface examinations showed that as the reinforcement ratio increased, the severity of surface damage decreased and abrasive wear mechanisms became more dominant. These findings demonstrate that hybrid reinforcement with TiC and MWCNT significantly enhances both mechanical and tribological performance, offering a promising alternative to additive manufacturing for Scalmalloy®-based composite production.

Keywords

• Scalmalloy^®
• hybrid composite
• mechanical
• tribological properties