Scientific Reports (Dec 2024)

A low-cost, open-source cylindrical Couette rheometer

  • Makita Erni,
  • A. John Hart,
  • David Trumper,
  • Crystal E. Owens

DOI
https://doi.org/10.1038/s41598-024-76494-8
Journal volume & issue
Vol. 14, no. 1
pp. 1 – 15

Abstract

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Abstract Rheology describes the flow of fluids from food and plastics, to coatings, adhesives, and 3D printing inks, and is commonly denoted by viscosity alone as a simplification. While viscometers adequately probe Newtonian (constant) viscosity, most fluids have complex viscosity, requiring tests over multiple shear rates, and transient measurements. As a result, rheometers are typically large, expensive, and require additional infrastructure (e.g., gas lines), rendering them inaccessible for regular use by many individuals, small organizations, and educators. Here, we introduce a low-cost (under USD$200 bill of materials) Open Source Rheometer (OSR), constructed entirely from thermoplastic 3D printed components and off-the-shelf electromechanical components. A sample fluid rests in a cup while a micro stepping motor rotates a tool inside the cup, applying strain-controlled shear flow. A loadcell measures reaction torque exerted on the cup, and viscosity is calculated. To establish the measurement range, the viscosity of four Newtonian samples of 0.1–10 Pa.s were measured with the OSR and compared to benchmark values from a laboratory rheometer, showing under 23% error. Building on this, flow curves of three complex fluids – a microgel (hand sanitizer), foam (Gillette), and biopolymer solution (1% Xanthan Gum) – were measured with a similar error range. Stress relaxation, a transient test, was demonstrated on the biopolymer solution to extract the nonlinear damping function. We finally include detailed exposition of measurement windows, sources of error, and future design suggestions. The OSR cost is ∼1/25th that of commercially available devices with comparable minimum torque (200 µN.m), and provides a fully open-source platform for further innovation in customized rheometry.