Methods to simplify cooling of liquid Helium cryostats
Rafael Álvarez Montoya,
Sara Delgado,
José Castilla,
José Navarrete,
Nuria Díaz Contreras,
Juan Ramón Marijuan,
Víctor Barrena,
Isabel Guillamón,
Hermann Suderow
Affiliations
Rafael Álvarez Montoya
Laboratorio de Bajas Temperaturas, Departamento de Física de la Materia Condensada, Instituto de Ciencia de Materiales Nicolás Cabrera and Condensed Matter Physics Center (IFIMAC), Facultad de Ciencias, Universidad Autónoma de Madrid, 28049 Madrid, Spain
Sara Delgado
Laboratorio de Bajas Temperaturas, Departamento de Física de la Materia Condensada, Instituto de Ciencia de Materiales Nicolás Cabrera and Condensed Matter Physics Center (IFIMAC), Facultad de Ciencias, Universidad Autónoma de Madrid, 28049 Madrid, Spain
José Castilla
Laboratorio de Bajas Temperaturas, Departamento de Física de la Materia Condensada, Instituto de Ciencia de Materiales Nicolás Cabrera and Condensed Matter Physics Center (IFIMAC), Facultad de Ciencias, Universidad Autónoma de Madrid, 28049 Madrid, Spain
José Navarrete
Segainvex, Universidad Autónoma de Madrid, 28049 Madrid, Spain
Nuria Díaz Contreras
Segainvex, Universidad Autónoma de Madrid, 28049 Madrid, Spain
Juan Ramón Marijuan
Segainvex, Universidad Autónoma de Madrid, 28049 Madrid, Spain
Víctor Barrena
Laboratorio de Bajas Temperaturas, Departamento de Física de la Materia Condensada, Instituto de Ciencia de Materiales Nicolás Cabrera and Condensed Matter Physics Center (IFIMAC), Facultad de Ciencias, Universidad Autónoma de Madrid, 28049 Madrid, Spain
Isabel Guillamón
Laboratorio de Bajas Temperaturas, Departamento de Física de la Materia Condensada, Instituto de Ciencia de Materiales Nicolás Cabrera and Condensed Matter Physics Center (IFIMAC), Facultad de Ciencias, Universidad Autónoma de Madrid, 28049 Madrid, Spain
Hermann Suderow
Laboratorio de Bajas Temperaturas, Departamento de Física de la Materia Condensada, Instituto de Ciencia de Materiales Nicolás Cabrera and Condensed Matter Physics Center (IFIMAC), Facultad de Ciencias, Universidad Autónoma de Madrid, 28049 Madrid, Spain; Corresponding author.
Liquid Helium is used widely, from hospitals to characterization of materials at low temperatures. Many experiments at low temperatures require liquid Helium, particularly when vibration isolation precludes the use of cryocoolers and when one needs to cool heavy equipment such as superconducting coils. Here we describe methods to simplify the operations required to use liquid Helium by eliminating the use of high pressure bottles, avoiding blockage and improving heating and cooling rates. First we show a simple and very low cost method to transfer liquid Helium from a transport container into a cryostat that uses a manual pump having pumping and pressurizing ports, giving a liquid Helium transfer rate of about 100 liters an hour. Second, we describe a closed cycle circuit of Helium gas cooled in an external liquid nitrogen bath that allows precooling a cryogenic experiment without inserting liquid nitrogen into the cryostat, eliminating problems associated to the presence of nitrogen around superconducting magnets. And third, we show a sliding seal assembly and an inner vacuum chamber design that allows inserting large experiments into liquid Helium. Keywords: Liquid Helium cryogenics, Superconducting solenoids, Cryogenic scanning probe microscopy, Materials characterization at low temperatures and high magnetic fields