Ibn Al-Haitham Journal for Pure and Applied Sciences (Apr 2017)

Synthesis And Characterization of 5-(Mercapto-1,3,4Thiadiazole-2yl)α,α-Diphenyl Methanol From Benzilic Acid

  • Muhanned J. Mahmoud,
  • Redha I. AL-bayati,
  • Shaimaa A. Saoud,
  • Ismaeel Y. Majeed

Journal volume & issue
Vol. 26, no. 1

Abstract

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5-(mercapto-1,3,4-thiadiazole-2yl)α,α-(diphenyl)methanol have been synthesized by ring closer of potassium xanthate[which have been prepared by reaction of benzilic acid hydrazide with carbon disulphide in potassium hydroxide] using conc.sulphuric acid at (0-5)°C scheme(I). Their characterization was carried out from T.L.C, M.P, FT.IR and 1H-NMR.

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