4-Phenyl-5a,6,7,8,9,9a-hexahydro-1H-1,5-benzodiazepin-2(5H)-one

Wedad Al Garadi; Youssef Ramli; Lhoussaine El Ghayati; Ahmed Moussaif; El Mokhtar Essassi; Joel T. Mague

doi:10.1107/S2414314618010118

IUCrData (Jul 2018)

4-Phenyl-5a,6,7,8,9,9a-hexahydro-1H-1,5-benzodiazepin-2(5H)-one

Wedad Al Garadi,
Youssef Ramli,
Lhoussaine El Ghayati,
Ahmed Moussaif,
El Mokhtar Essassi,
Joel T. Mague

Affiliations

Wedad Al Garadi: Laboratoire de Chimie Organique Heterocyclique URAC 21, Av. Ibn Battouta, BP 1014, Faculte des Sciences, Universite Mohammed V, Rabat, Morocco
Youssef Ramli: Laboratory of Medicinal Chemistry, Drug Sciences Research Center, Faculty of Medicine and Pharmacy, Mohammed V University, Rabat, Morocco
Lhoussaine El Ghayati: Laboratoire de Chimie Organique Heterocyclique URAC 21, Av. Ibn Battouta, BP 1014, Faculte des Sciences, Universite Mohammed V, Rabat, Morocco
Ahmed Moussaif: National Center of Energy Sciences and Nuclear Techniques, Rabat, Morocco
El Mokhtar Essassi: Laboratoire de Chimie Organique Heterocyclique URAC 21, Av. Ibn Battouta, BP 1014, Faculte des Sciences, Universite Mohammed V, Rabat, Morocco
Joel T. Mague: Department of Chemistry, Tulane University, New Orleans, LA 70118, USA

DOI: https://doi.org/10.1107/S2414314618010118
Journal volume & issue: Vol. 3, no. 7
p. x181011

Abstract

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In the title compound, C15H18N2O, the cyclohexyl portion is disordered over two alternate chair conformations in a 0.911 (2):0.089 (2) ratio. In the crystal, inversion-related pairwise N—H...O hydrogen bonds form dimers, which are connected into (100) layers by additional N—H...O hydrogen bonds.

Published in IUCrData

ISSN: 2414-3146 (Online)
Publisher: International Union of Crystallography
Country of publisher: United Kingdom
LCC subjects: Science: Chemistry: Crystallography
Website: https://iucrdata.iucr.org

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