Brazilian Journal of Radiation Sciences (Jun 2020)

Optimization of the gamma-ray spectrometry counting time based on uncertainties of radionuclides concentration in samples

  • Marcelo Bessa Nisti,
  • Marcelo Francis Máduar,
  • Catia Heloisa Rosignoli Saueia,
  • Fernanda Cavalcante,
  • Barbara Paci Mazzilli

DOI
https://doi.org/10.15392/bjrs.v8i2.1197
Journal volume & issue
Vol. 8, no. 2

Abstract

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This paper aims to propose an easy and fast method of optimization of the gamma-ray spectrometry counting time in determining natural radionuclides (Pb-210, Pb-212, Pb-214, Bi-212, Bi-214 and Ac-228) in order to minimize uncertainties in the concentration. The samples were measured by gamma-ray spectrometry with a hyper-pure germanium detector Canberra, 25% relative efficiency, effective resolution of 1.9 keV on the 1332.5 keV 60Co with associated electronics and coupled to a microcomputer. Multichannel Maestro A65-I model was used for spectrum acquisition and peak net area determination, and WinnerGamma/Interwinner 6.01 software was used for gamma-ray spectra analysis and to calculate the concentrations and associated uncertainties. The counting times used were 86,000 s and 150,000 s.

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