4-(Furan-2-carbonyl)piperazin-1-ium 3,5-dinitrobenzoate

Channappa N. Kavitha; Manpreet Kaur; Jerry P. Jasinski; Ray J. Butcher; H.S. Yathirajan

doi:10.1107/S160053681401126X

Acta Crystallographica Section E (Jun 2014)

4-(Furan-2-carbonyl)piperazin-1-ium 3,5-dinitrobenzoate

Channappa N. Kavitha,
Manpreet Kaur,
Jerry P. Jasinski,
Ray J. Butcher,
H.S. Yathirajan

Affiliations

Channappa N. Kavitha: Department of Studies in Chemistry, University of Mysore, Manasagangotri, Mysore 570 006, India
Manpreet Kaur: Department of Studies in Chemistry, University of Mysore, Manasagangotri, Mysore 570 006, India
Jerry P. Jasinski: Department of Chemistry, Keene State College, 229 Main Street, Keene, NH 03435-2001, USA
Ray J. Butcher: Department of Chemistry, Howard University, 525 College Street NW, Washington, DC 20059, USA
H.S. Yathirajan: Department of Studies in Chemistry, University of Mysore, Manasagangotri, Mysore 570 006, India

DOI: https://doi.org/10.1107/S160053681401126X
Journal volume & issue: Vol. 70, no. 6
pp. o700 – o701

Abstract

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In the cation of the title salt, C9H13N2O2+·C7H3N2O6−, the piperazine ring adopts a slightly distorted chair conformation. Twofold rotational disorder is exhibited by the furan ring in a 0.430 (4):0.570 (4) ratio. In the crystal, N—H...O hydrogen bonds link the ions into chains along [010]. Additional weak C—H...O interactions are observed, leading to a supramolecular layer parallel to (011).

Published in Acta Crystallographica Section E

ISSN: 1600-5368 (Online)
Publisher: International Union of Crystallography
Country of publisher: United Kingdom
LCC subjects: Science: Chemistry: Crystallography
Website: https://journals.iucr.org/e/

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