Scientific Reports (Sep 2023)

Multi-directional neutron dark-field imaging with single absorption grating

  • Matteo Busi,
  • Jiazhou Shen,
  • Michael Bacak,
  • Marie Christine Zdora,
  • Jan Čapek,
  • Jacopo Valsecchi,
  • Markus Strobl

DOI
https://doi.org/10.1038/s41598-023-42310-y
Journal volume & issue
Vol. 13, no. 1
pp. 1 – 7

Abstract

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Abstract Neutron dark-field imaging is a powerful technique for investigating the microstructural properties of materials through high-resolution full-field mapping of small-angle scattering. However, conventional neutron dark-field imaging utilizing Talbot–Lau interferometers is limited to probing only one scattering direction at a time. Here, we introduce a novel multi-directional neutron dark-field imaging approach that utilizes a single absorption grating with a two-dimensional pattern to simultaneously probe multiple scattering directions. The method is demonstrated to successfully resolve fiber orientations in a carbon compound material as well as the complex morphology of the transformed martensitic phase in additively manufactured stainless steel dogbone samples after mechanical deformation. The latter results reveal a preferential alignment of transformed domains parallel to the load direction, which is verified by EBSD. The measured real-space correlation functions are in good agreement with those extracted from the EBSD map. Our results demonstrate that multi-directional neutron dark-field imaging is overcoming significant limitations of conventional neutron dark-field imaging in assessing complex heterogeneous anisotropic microstructures and providing quantitative structural information on multiple length scales.