Química Nova (Jan 2012)

Biomassa em aula prática de Química Orgânica Verde: cravo-da-índia como fonte simultânea de óleo essencial e de furfural

  • Silvio Cunha,
  • Danilo Machado Lustosa,
  • Nathan Dias Conceição,
  • Miguel Fascio,
  • Vinícius Magalhães

DOI
https://doi.org/10.1590/S0100-40422012000300035
Journal volume & issue
Vol. 35, no. 3
pp. 638 – 641

Abstract

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This work presents an optimized integrated experiment for isolation of clove bud essential oil, rich in eugenol, and subsequent utilization of the solid residue for furfural synthesis. The operationally simple laboratory protocols and utilization of water as a solvent in both operations, plus the use of biomass as the starting material for preparation of versatile intermediates in organic synthesis, make the experiments attractive for undergraduate experimental organic chemistry courses in the context of green chemistry. In addition, this is the first description of the use of biomass (clove bud) in the simultaneous preparation of two chemical feedstocks, eugenol and furfural, on experimental organic chemistry courses.

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