Materials (Jun 2021)

Ni/Al-Hybrid Cellular Foams: An Interface Study by Combination of 3D-Phase Morphology Imaging, Microbeam Fracture Mechanics and In Situ Synchrotron Stress Analysis

  • Jutta Luksch,
  • Anne Jung,
  • Christoph Pauly,
  • Ralf Derr,
  • Patrick Gruenewald,
  • Marc Laub,
  • Manuela Klaus,
  • Christoph Genzel,
  • Christian Motz,
  • Frank Mücklich,
  • Florian Schaefer

DOI
https://doi.org/10.3390/ma14133473
Journal volume & issue
Vol. 14, no. 13
p. 3473

Abstract

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Nickel(Ni)/aluminium(Al) hybrid foams are Al base foams coated with Ni by electrodeposition. Hybrid foams offer an enhanced energy absorption capacity. To ensure a good adhering Ni coating, necessary for a shear resistant interface, the influence of a chemical pre-treatment of the base foam was investigated by a combination of an interface morphology analysis by focused ion beam (FIB) tomography and in situ mechanical testing. The critical energy for interfacial decohesion from these microbending fracture tests in the scanning electron microscope (SEM) were contrasted to and the results validated by depth-resolved measurements of the evolving stresses in the Ni coating during three-point bending tests at the energy-dispersive diffraction (EDDI) beamline at the synchrotron BESSY II. Such a multi-method assessment of the interface decohesion resistance with respect to the interface morphology provides a reliable investigation strategy for further improvement of the interface morphology.

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