Synthesis and Characterisation of Hydroxyl-terminated Liquid Natural Rubber by Photo-Fenton Reaction

H. L. Pham; B. T. Do; T. S. Pham; D. G. Le

doi:10.29037/ajstd.347

ASEAN Journal on Science and Technology for Development (Dec 2017)

Synthesis and Characterisation of Hydroxyl-terminated Liquid Natural Rubber by Photo-Fenton Reaction

H. L. Pham,
B. T. Do,
T. S. Pham,
D. G. Le

Affiliations

H. L. Pham: Institute of Chemistry, Vietnam Academy of Science and Technology, 18-Hoang Quoc Viet Road, Cau Giay District, Hanoi, Vietnam
B. T. Do: Institute of Chemistry, Vietnam Academy of Science and Technology, 18-Hoang Quoc Viet Road, Cau Giay District, Hanoi, Vietnam
T. S. Pham: Institute of Chemistry, Vietnam Academy of Science and Technology, 18-Hoang Quoc Viet Road, Cau Giay District, Hanoi, Vietnam
D. G. Le: University of Vinh, Nghean, Vietnam

DOI: https://doi.org/10.29037/ajstd.347
Journal volume & issue: Vol. 30, no. 1&2
pp. 29 – 36

Abstract

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Hydroxyl-terminated liquid natural rubber (HTNR) was prepared by the photo-Fenton reaction, which was carried out in solution in the presence of H2O2/Fe(II) combined with UV irradiation. The HTNR obtained was characterized by GPC, FT-IR, 1H-NMR, 13C-NMR, DEPT-NMR spectroscopy as well as by chemical methods. A probable mechanism leading to the formation of HTNR was discussed based on the analytical data.

Published in ASEAN Journal on Science and Technology for Development

ISSN: 0217-5460 (Print); 2224-9028 (Online)
Publisher: Universiti Brunei Darussalam
Country of publisher: Brunei Darussalam
LCC subjects: Technology: Technology (General); Science: Science (General)
Website: https://ajstd.ubd.edu.bn/journal/

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