Acta Crystallographica Section E (Jul 2013)

1,5-Bis(2-methoxybenzylidene)thiocarbonohydrazide methanol monosolvate

  • Jianfeng Yu,
  • Shiming Tang,
  • Jingbin Zeng,
  • Zifeng Yan

DOI
https://doi.org/10.1107/S1600536813016954
Journal volume & issue
Vol. 69, no. 7
pp. o1147 – o1147

Abstract

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The title compound, C17H18N4O2S·CH3OH, was synthesized by the condensation reaction of o-methoxybenzaldehyde with thiocarbohydrazide in methanol. The two benzene rings are inclined each to other at 31.7 (1)°. Intermolecular N—H...O and bifurcated O—H...N(S) hydrogen bonds link two thiocarbonohydrazide and two solvent molecules into a centrosymmetric unit. These units, related by translation along the b axis, are further aggregated into columns through N—H...S hydrogen bonds.