Determinação de paládio em amostras biológicas aplicando técnicas analíticas nucleares Determination of palladium in biological samples applying nuclear analytical techniques

Abstract

This study presents Pd determinations in bovine tissue samples containing palladium prepared in the laboratory, and CCQM-P63 automotive catalyst materials of the Proficiency Test, using instrumental thermal and epithermal neutron activation analysis and energy dispersive X-ray fluorescence techniques. Solvent extraction and solid phase extraction procedures were also applied to separate Pd from interfering elements before the irradiation in the nuclear reactor. The results obtained by different techniques were compared against each other to examine sensitivity, precision and accuracy.

Keywords

• nuclear analytical techniques
• palladium
• biological samples