Molecules (May 2009)

Silica Bonded S-Sulfonic Acid: A Recyclable Catalyst for the Synthesis of Quinoxalines at Room Temperature

  • Khodabakhsh Niknam,
  • Maleki Mohagheghnejad,
  • Dariush Saberi

DOI
https://doi.org/10.3390/molecules14051915
Journal volume & issue
Vol. 14, no. 5
pp. 1915 – 1926

Abstract

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The reaction of 3-mercaptopropylsilica (MPS) and chlorosulfonic acid in chloroform afforded silica bonded S-sulfonic acid (SBSSA), which was used as a catalyst for the room temperature synthesis of quinoxaline derivatives from 1,2-diamino compounds and 1,2-dicarbonyl compounds. The catalyst could be recycled and reused several times without any loss of efficiency.

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