Zeitschrift für Kristallographie - New Crystal Structures (Jun 2023)
The crystal structure of di-μ-1-naphthylacetato-κ 3 O,O′:O;κ 3 O:O,O′-bis[(1-naphthylacetato-κ 2 O,O′)(2,2′-bipyridine-κ 2 N,N′)lead(II)] monohydrate, C68H54N4O9Pb2
Abstract
C68H54N4O9Pb2 ${\mathrm{C}}_{68}{\mathrm{H}}_{54}{\mathrm{N}}_{4}{\mathrm{O}}_{9}{\mathrm{P}\mathrm{b}}_{2}$ , monoclinic, C2/c (no. 15), a = 15.7286(14) Å, b = 16.3623(14) Å, c = 22.500(2) Å, β = 97.369(1)° $97.369(1){}^{\circ}$ , V = 5742.7(9) Å3 ${\mathrm{\mathring{\text{A}}}}^{3}$ , Z = 4, Rgt ${R}_{gt}$ (F) = 0.0203, w Rref ${R}_{ref}$ (F2 ${F}^{2}$ ) = 0.0488, T = 296(2) K.
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