The Effect of Glazing and Repeated Firing on Color, Translucency, and Flexural Strength of Different Types of Zirconia: An In Vitro Study

Abstract

This study evaluated the impact of glazing and multiple firing on the flexural strength, translucency, and color stability of three types of zirconia: 3 mol% yttria-stabilized tetragonal zirconia polycrystals (3Y-TZP), 4 mol% yttria partially stabilized zirconia (4Y-PSZ), and 5 mol% yttria partially stabilized zirconia (5Y-PSZ). A total of 120 samples were categorized into four groups: polishing only (P), polishing + glazing (PG), polishing + glazing + one glaze firing (PGF), and polishing + glazing + two glaze firings (PGFF). A three-point bending test was used for assessing flexural strength and a spectrophotometer analysis for assessing color difference (ΔE*ab) and translucency parameter (TP). Statistical analysis included one-way ANOVA and Kruskal–Wallis tests, with significance set at α = 0.05. The type 3Y-TZP showed the highest flexural strength (918.46 MPa) and lowest translucency (TP = 4.32), while 5Y-PSZ exhibited the lowest strength (401.58 MPa, p p ≤ 0.012). Heat treatment resulted in a significant reduction in the flexural strength of 5Y-PSZ (p = 0.002), followed by 3Y-TZP (p = 0.04). The type 5Y-PSZ exhibited significant change in translucency (p = 0.003) and unacceptable variations in color (ΔE*ab: 1.49–9.6). The type 4Y-PSZ exhibited the highest stability in flexural strength, translucency, and color under multiple treatments. In conclusion, while glazing and firing significantly compromised 5Y-PSZ’s flexural strength and altered its color and translucency, 4Y-PSZ demonstrated the highest stability.

Keywords

• zirconia
• flexural strength
• translucency
• color stability
• heat treatment