Data analysis of “krokodil” samples obtained by street-like synthesis
João Filipe Neves,
Emanuele Amorim Alves,
José Xavier Soares,
Sara Manuela Cravo,
Artur M.S. Silva,
Annibal Duarte Pereira Netto,
Félix Carvalho,
Ricardo Jorge Dinis-Oliveira,
Carlos Manuel Afonso
Affiliations
João Filipe Neves
Department of Chemical Sciences, Laboratory of Organic and Pharmaceutical Chemistry, Faculty of Pharmacy, University of Porto, Porto, Portugal
Emanuele Amorim Alves
UCIBIO-REQUIMTE, Laboratory of Toxicology, Department of Biological Sciences, Faculty of Pharmacy, University of Porto, Porto, Portugal; Department of Legal Medicine and Forensic Sciences, Faculty of Medicine, University of Porto, Porto, Portugal; EPSJV – Polytechnic School of Health Joaquim Venâncio, Oswaldo Cruz Foundation, Rio de Janeiro, Brazil; Corresponding authors at: UCIBIO-REQUIMTE, Laboratory of Toxicology, Department of Biological Sciences, Faculty of Pharmacy, University of Porto, Porto, Portugal, Rua José Viterbo Ferreira no. 228 4050-313, Porto, Portugal. Tel.: +351 220428597.
José Xavier Soares
LAQV-REQUIMTE, Department of Chemical Sciences, Laboratory of Applied Chemistry, Faculty of Pharmacy, University of Porto, Porto, Portugal
Sara Manuela Cravo
Department of Chemical Sciences, Laboratory of Organic and Pharmaceutical Chemistry, Faculty of Pharmacy, University of Porto, Porto, Portugal
Artur M.S. Silva
Department of Chemistry and QOPNA, University of Aveiro, Campus Universitário de Santiago, Aveiro, Portugal
Annibal Duarte Pereira Netto
Department of Analytical Chemistry, Chemistry Institute, Fluminense Federal University, Niterói, Brazil
Félix Carvalho
UCIBIO-REQUIMTE, Laboratory of Toxicology, Department of Biological Sciences, Faculty of Pharmacy, University of Porto, Porto, Portugal
Ricardo Jorge Dinis-Oliveira
UCIBIO-REQUIMTE, Laboratory of Toxicology, Department of Biological Sciences, Faculty of Pharmacy, University of Porto, Porto, Portugal; Department of Legal Medicine and Forensic Sciences, Faculty of Medicine, University of Porto, Porto, Portugal; IINFACTS-Institute of Research and Advanced Training in Health Sciences and Technologies, Department of Sciences, University Institute of Health Sciences (IUCS), CESPU, CRL, Gandra, Portugal; Corresponding authors at: UCIBIO-REQUIMTE, Laboratory of Toxicology, Department of Biological Sciences, Faculty of Pharmacy, University of Porto, Porto, Portugal, Rua José Viterbo Ferreira no. 228 4050-313, Porto, Portugal. Tel.: +351 220428597.
Carlos Manuel Afonso
Department of Chemical Sciences, Laboratory of Organic and Pharmaceutical Chemistry, Faculty of Pharmacy, University of Porto, Porto, Portugal; Interdisciplinary Center of Marine and Environmental Investigation (CIIMAR/CIMAR), Porto, Portugal; Corresponding author at: Department of Chemical Sciences, Laboratory of Organic and Pharmaceutical Chemistry, Faculty of Pharmacy, University of Porto.
The data described in this work is related to be the subject of an article in the Forensic Science International, titled: “The harmful chemistry behind “krokodil”: street-like synthesis and product analysis” (http://dx.doi.org/10.1016/j.forsciint.2015.07.042) [1]. The data presented here provides additional description of the chemical profile of “krokodil”. Physicochemical and organoleptic characteristics, TLC profile, UV/Vis, 1H NMR and FTIR spectrum are presented. These data validate the proposed synthetic procedure and pathway and give further information about the contaminants present in “krokodil”. Keywords: “Krokodil”, Street like synthesis, TLC profile, UV/Vis, 1H NMR, FTIR
