Crystals (Dec 2024)

A Concept of an Educational Multi-Technique Beamline for Crystalline Matter Studies at Synchrotron Radiation Facility SKIF

  • Alexander Selyutin,
  • Denis Mishchenko,
  • Zakhar Vinokurov,
  • Olga Bulavchenko,
  • Andrey Saraev,
  • Sergey Tsybulya,
  • Yan Zubavichus

DOI
https://doi.org/10.3390/cryst14121056
Journal volume & issue
Vol. 14, no. 12
p. 1056

Abstract

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A concept of a high throughput, user-friendly, versatile bending magnet beamline at the fourth-generation synchrotron radiation facility SKIF, currently being constructed in Koltsovo (a science town near Novosibirsk, Russia), is proposed. The beamline is designed to implement the conventional and most demanded synchrotron techniques: XAS (X-ray absorption spectroscopy); XRD (X-ray diffraction), both powder and single-crystal, including the in situ mode; and XRF (X-ray fluorescence analysis). The beamline is conceived to be as simple as possible, but it is multifunctional, being a base beamline for the education and training of students, future synchrotron users, and beamline scientists. A number of potential beamline optical layouts are modeled in the XRT (XRayTracer) program package. The resulting beam characteristics at the sample position are discussed. A monochromator model is proposed. Surface distortions and their influence on the rocking curve of the Si111 crystal due to incoming heat loads are realistically modeled. The optimum design of the station is defined. The range of crystalline objects that are possible to be studied at the proposed station is emphasized, and future perspectives are outlined.

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