Study on synthesis of the perfume ionone(香料紫罗兰酮的合成研究)

SUNQing(孙青); SHUXue-jun(舒学军); CHENRu-bing(陈茹冰); YINXu-guang(殷旭光); WANGBo(王波)

doi:10.3785/j.issn.1008-9497.2012.01.012

Zhejiang Daxue xuebao. Lixue ban (Jan 2012)

Study on synthesis of the perfume ionone(香料紫罗兰酮的合成研究)

SUNQing(孙青),
SHUXue-jun(舒学军),
CHENRu-bing(陈茹冰),
YINXu-guang(殷旭光),
WANGBo(王波)

Affiliations

SUNQing(孙青): College of Chemistry and Chemical Engineering, Jiangxi Normal University, Nanchang 330022, China(江西师范大学化学化工学院，江西南昌 330022)
SHUXue-jun(舒学军): College of Chemistry and Chemical Engineering, Jiangxi Normal University, Nanchang 330022, China(江西师范大学化学化工学院，江西南昌 330022)
CHENRu-bing(陈茹冰): College of Chemistry and Chemical Engineering, Jiangxi Normal University, Nanchang 330022, China(江西师范大学化学化工学院，江西南昌 330022)
YINXu-guang(殷旭光): College of Chemistry and Chemical Engineering, Jiangxi Normal University, Nanchang 330022, China(江西师范大学化学化工学院，江西南昌 330022)
WANGBo(王波): College of Chemistry and Chemical Engineering, Jiangxi Normal University, Nanchang 330022, China(江西师范大学化学化工学院，江西南昌 330022)

DOI: https://doi.org/10.3785/j.issn.1008-9497.2012.01.012
Journal volume & issue: Vol. 39, no. 1
pp. 56 – 59

Abstract

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报道用新的催化剂合成紫罗兰酮.用CH3ONa作固体碱催化剂催化柠檬醛与丙酮的Aldol缩合反应，在50〜60℃反应3. 5 h，以95. 3%的收率制得假性紫罗兰酮，然后假性紫罗兰酮在磷酸催化下进行关环反应，于温度55〜65℃反应，得质量分数为97. 6%的紫罗兰酮，收率81. 5%，对合成条件进行了分析和讨论，对产品紫罗兰酮的IR谱图、NMR谱图进行了确认和详细的分析.

Published in Zhejiang Daxue xuebao. Lixue ban

ISSN: 1008-9497 (Print)
Publisher: Zhejiang University Press
Country of publisher: China
LCC subjects: Science: Mathematics: Instruments and machines: Electronic computers. Computer science; Science: Physics
Website: https://www.zjujournals.com/sci/EN/1008-9497/home.shtml

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