N′-(3-Bromo-7-oxo-7H-benzo[de]anthracen-9-yl)-N,N-dimethylimidoformamide

Evita Romanovska; Aleksandrs Pučkins; Tatjana Grigorjeva; Elena Kirilova

doi:10.3390/M1323

Molbank (Jan 2022)

N′-(3-Bromo-7-oxo-7H-benzo[de]anthracen-9-yl)-N,N-dimethylimidoformamide

Evita Romanovska,
Aleksandrs Pučkins,
Tatjana Grigorjeva,
Elena Kirilova

Affiliations

Evita Romanovska: Department of Applied Chemistry, Institute of Life Sciences and Technology, Daugavpils University, 1A Parades Street, LV-5401 Daugavpils, Latvia
Aleksandrs Pučkins: Department of Applied Chemistry, Institute of Life Sciences and Technology, Daugavpils University, 1A Parades Street, LV-5401 Daugavpils, Latvia
Tatjana Grigorjeva: Department of Applied Chemistry, Institute of Life Sciences and Technology, Daugavpils University, 1A Parades Street, LV-5401 Daugavpils, Latvia
Elena Kirilova: Department of Applied Chemistry, Institute of Life Sciences and Technology, Daugavpils University, 1A Parades Street, LV-5401 Daugavpils, Latvia

DOI: https://doi.org/10.3390/M1323
Journal volume & issue: Vol. 2022, no. 1
p. M1323

Abstract

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We report a synthesis of 3-bromo-9-N′-(N,N-dimethylformamidino)benzanthrone in good yield by a condensation reaction of 3-bromo-9-aminobenzanthrone with dimethylformamide in the presence of phosphorous oxychloride. The structure of the synthesized amidine was characterized by FTIR-ATR, NMR experiments, and elemental analysis. The title compound was analyzed by UV-Vis and fluorescence spectroscopy in various organic solvents.

Published in Molbank

ISSN: 1422-8599 (Online)
Publisher: MDPI AG
Country of publisher: Switzerland
LCC subjects: Science: Chemistry: Inorganic chemistry
Website: https://www.mdpi.com/journal/molbank

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