Synthesis, characterization and thermal studies on solid state 3-methoxybenzoate of lighter trivalent lanthanides

Patrícia Roberta Dametto; A. B. Siqueira; C. T. Carvalho; Massao Ionashiro

doi:10.26850/1678-4618eqj.v32.2.2007.p17-21

Eclética Química (Sep 2018)

Synthesis, characterization and thermal studies on solid state 3-methoxybenzoate of lighter trivalent lanthanides

Patrícia Roberta Dametto,
A. B. Siqueira,
C. T. Carvalho,
Massao Ionashiro

Affiliations

Patrícia Roberta Dametto: Instituto de Química, UNESP, C. P. 355, CEP 14801 – 970, Araraquara, SP, Brazil.
A. B. Siqueira: Instituto de Química, UNESP, C. P. 355, CEP 14801 – 970, Araraquara, SP, Brazil.
C. T. Carvalho: Instituto de Química, UNESP, C. P. 355, CEP 14801 – 970, Araraquara, SP, Brazil.
Massao Ionashiro: Instituto de Química, UNESP, C. P. 355, CEP 14801 – 970, Araraquara, SP, Brazil.

DOI: https://doi.org/10.26850/1678-4618eqj.v32.2.2007.p17-21
Journal volume & issue: Vol. 32, no. 2
pp. 17 – 21

Abstract

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Solid-state Ln -3-MeO-Bz compounds, where Ln stands for lighter trivalent lanthanides (La – Sm) and 3-methoxybenzoate, have been synthesized. Thermogravimetry (TG), differential scanning calorimetry (DSC), X-ray powder diffractometry, infrared spectroscopy, and complexometry were used to characterize and to study the thermal behaviour of these compounds. The results led to information concerning the composition, dehydration, polymorphic transformation, thermal behaviour and thermal decomposition of the synthesized compounds.

Published in Eclética Química

ISSN: 0100-4670 (Print); 1678-4618 (Online)
Publisher: Universidade Estadual Paulista
Country of publisher: Brazil
LCC subjects: Science: Chemistry
Website: http://revista.iq.unesp.br/ojs/index.php/ecletica/

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