Jurnal Riset Kimia (Mar 2020)

Struktur dan Sifat Dielektrik Senyawa Aurivillius CaBi3LaTi4O15 yang Disintesis dengan Teknik Hidrotermal

  • Zulhadjri Zulhadjri,
  • Firmanul Qadri Amir,
  • Marsal Mahmud,
  • Upita Septiani,
  • Syukri Arief

DOI
https://doi.org/10.25077/jrk.v11i1.343
Journal volume & issue
Vol. 11, no. 1
pp. 9 – 15

Abstract

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Synthesis of four-layer Aurivillius CaBi3LaTi4O15 has been successfully carried out by hydrothermal technique using NaOH 4 M as mineralizer. The reaction was carried out at 220 °C for 72 h. Crystal structure, morphology, and dielectric properties were analyzed in this study. X-ray diffraction confirmed that the single-phase product was successfully obtained. The refinement result shows the product has orthorhombic crystal structure with space group A21am. The morphology analyzed using SEM shows plate-like grains are observed, which is characteristic of Aurivillius phase. Dielectric curves show peaks at 585 °C which indicate ferroelectric transition temperature.

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