Journal of Materials Research and Technology (Jul 2023)
Microstructure and texture evolutions in FeCrAl cladding tube during pilger processing
Abstract
The microstructure of FeCrAl cladding tubes depends on the fabricating process history. In this study, the microstructural characteristics of wrought FeCrAl alloys during industrial pilger processing into thin-walled tubes were investigated. The hot extruded tube showed ∼100 μm equiaxed grains with weak α∗-fiber in {h11} texture, while pilger rolling process change the microstructure to fragmented and elongated grains along the rolling direction. The pilgered textures could be predicted with the VPSC model. The inter-pass annealing at 800–850 °C for 1 h results in recovery and recrystallization of the ferric matrix and restoration of ductility. The final finished tube shows fine recrystallized grains (∼11 μm) with dominant γ-fiber in three dimensions. Pilger rolling enhanced α-fiber while annealing reduced α-fiber and enhanced γ-fiber. Microstructural evolution in the Laves precipitates followed the sequence of faceted needle-like → spherical → faceted ellipsoidal. Thermomechanical processing resulted in cladding tubes with an area fraction of ∼5% and a number density of 5 × 10−11 m−2 in Laves precipitates, which is half that of the first-pilgered tube. Laves precipitates pin the grain boundaries to control the microstructure and prevent grain coarsening.