Molbank
(Jan 2023)
(<i>S</i>)-<i>N</i><sup>1</sup>,<i>N</i><sup>3</sup>-Dibenzyl-1-cyclohexyl-<i>N</i><sup>1</sup>,<i>N</i><sup>3</sup>-bis((<i>R</i>)-1-phenylethyl)propane-1,3-diamine
Leland Belda,
Ángel García-González,
Alejandro Manchado,
Carlos T. Nieto,
Narciso M. Garrido
Affiliations
Leland Belda
Department of Organic Chemistry, Faculty of Chemical Sciences, University of Salamanca, Pl. Caídos, s/n, 37008 Salamanca, Spain
Ángel García-González
Department of Organic Chemistry, Faculty of Chemical Sciences, University of Salamanca, Pl. Caídos, s/n, 37008 Salamanca, Spain
Alejandro Manchado
Department of Organic Chemistry, Faculty of Chemical Sciences, University of Salamanca, Pl. Caídos, s/n, 37008 Salamanca, Spain
Carlos T. Nieto
Department of Organic Chemistry, Faculty of Chemical Sciences, University of Salamanca, Pl. Caídos, s/n, 37008 Salamanca, Spain
Narciso M. Garrido
Department of Organic Chemistry, Faculty of Chemical Sciences, University of Salamanca, Pl. Caídos, s/n, 37008 Salamanca, Spain
DOI
https://doi.org/10.3390/M1544
Journal volume & issue
Vol. 2023,
no. 1
Abstract
Read online
(S)-N1,N3-dibenzyl-1-cyclohexyl-N1,N3-bis((R)-1-phenylethyl)propane-1,3-diamine was prepared in good yield by the reduction of the corresponding amide, which was obtained by the addition of a chiral lithium amide to an α,β-unsaturated ester. The target compound was fully characterized by NMR (1H and 13C), high-resolution mass spectrometry and polarimetry.
Keywords
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