Molbank (Oct 2016)

4-Acetyl-2-hydroxy-2,5-dimethylfuran-3(2H)-one

  • Chiaki Akazaki,
  • Shun Kawabata,
  • Hiroshi Nishino

DOI
https://doi.org/10.3390/M913
Journal volume & issue
Vol. 2016, no. 4
p. M913

Abstract

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The facile synthesis of 4-acetyl-2-hydroxy-2,5-dimethylfuran-3(2H)-one (4) was achieved by the Mn(OAc)3-mediated aerobic oxidation of 2,4-pentanedione or the direct reaction of Mn(acac)3 in AcOH-TFE at room temperature under a dried air stream.

Keywords