Zeitschrift für Kristallographie - New Crystal Structures (Aug 2023)
The crystal structure of fac-tricarbonyl(2-pyridin-2-yl-quinoline-κ2 N,N′)-(pyrazole-κN)rhenium(I)nitrate, C20H14N4O3ReNO3
Abstract
C20H14N4O3 ${\mathrm{C}}_{20}{\mathrm{H}}_{14}{\mathrm{N}}_{4}{\mathrm{O}}_{3}$ ReNO3 ${\mathrm{N}\mathrm{O}}_{3}$ , monoclinic, P21 ${2}_{1}$ /c (no. 14), a = 12.9572 (2), b = 9.1568 (2), c = 17.3658 (3) Å, β = 97.267(2)° $97.267(2){}^{\circ}$ , V = 2043.84 (7) Å3 ${\mathrm{\mathring{\text{A}}}}^{3}$ , Z = 4, Rgt ${R}_{gt}$ (F) = 0.0231, wRref $w{R}_{ref}$ (F2 ${F}^{2}$ ) = 0.0514, T = 154 K
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