Kirkuk Journal of Science (Dec 2016)

Preparation and diagnosis some heterocyclic compounds that derived from 1,3,4 – Thiadiazole compound derived from 1,3,4 – Thiadiazole compound

  • Ayad S. H. AL-Maaini Nazhan.KA AL-Luhiby

DOI
https://doi.org/10.32894/kujss.2016.131072
Journal volume & issue
Vol. 11, no. 4
pp. 184 – 197

Abstract

Read online

This search included synthesis of some heterocyclic compounds devired from 1,3,4- thiadiazol ring ,such as thaiazolidin -4-one substituents Azetidine -3- one and Azo dyes. These compounds were aprepard from Shiff bases loaded on thiazdiazol ring, These bases have been treated with Aniline substituents in presence of pyrididine as a catalyst to give azo dyes , thioglycolic acid to produce thiazolidine -4- one in presence of ZnCl2 as catalyst and finally with chloroacetylchloride to produce Azetidine-3-one in presence of tryethylamine as a catalyst. The prepared compounds were identifie by physical properties and IR,H1-NMR Spectroscopy.

Keywords