Data on validation using accuracy profile of HPLC-UV method

Ahmed M. Ibrahim; Hassan A.M. Hendawy; Wafaa S. Hassan; Abdalla Shalaby; Heba M. El-sayed

Data in Brief (Jun 2019)

Data on validation using accuracy profile of HPLC-UV method

Ahmed M. Ibrahim,
Hassan A.M. Hendawy,
Wafaa S. Hassan,
Abdalla Shalaby,
Heba M. El-sayed

Affiliations

Ahmed M. Ibrahim: National Organization for Drug Control and Research, P.O. Box 29, Cairo, Egypt; Corresponding author.
Hassan A.M. Hendawy: National Organization for Drug Control and Research, P.O. Box 29, Cairo, Egypt
Wafaa S. Hassan: Department of Analytical Chemistry, Faculty of Pharmacy, Zagazig University, Zagazig, Egypt
Abdalla Shalaby: Department of Analytical Chemistry, Faculty of Pharmacy, Zagazig University, Zagazig, Egypt
Heba M. El-sayed: Department of Analytical Chemistry, Faculty of Pharmacy, Zagazig University, Zagazig, Egypt

Journal volume & issue: Vol. 24

Abstract

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The data presented are related to the article entitled “Six Sigma quality approach for HPLC-UV method optimization” Ibrahim et al., 2019. The raw data of HPLC analysis of ascorbic acid (AS), paracetamol (PA) and guaifenesin (GU) are presented. Calibration standards were prepared at six concentrations levels (25%, 50%, 75%, 100%, 125% and 150%) each day and measured in triplicate. Validation standards were prepared at four concentration levels (25%, 60%, 100% and 150%) each day and measured in quintet. Three different series were used for method validation and prepared at the rate of one series per day. Keywords: Accuracy profile, HPLC, Ascorbic acid, Paracetamol, Guaifenesin

Published in Data in Brief

ISSN: 2352-3409 (Online)
Publisher: Elsevier
Country of publisher: United States
LCC subjects: Medicine: Medicine (General): Computer applications to medicine. Medical informatics; Science: Science (General)
Website: http://www.journals.elsevier.com/data-in-brief/

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