Superalloy/Al2O3 type composite compacts obtained by spark plasma sintering from mechanically alloyed powders

Prică Călin V.; Sechel Niculina A.; Neamțu Bogdan V.; Marinca Traian F.; Popa Florin; Chicinaș Horea F.; Chicinaș Ionel

doi:10.2298/SOS2203335P

Science of Sintering (Jan 2022)

Superalloy/Al2O3 type composite compacts obtained by spark plasma sintering from mechanically alloyed powders

Prică Călin V.,
Sechel Niculina A.,
Neamțu Bogdan V.,
Marinca Traian F.,
Popa Florin,
Chicinaș Horea F.,
Chicinaș Ionel

Affiliations

Prică Călin V.: Materials Science and Engineering Department, Technical University of Cluj-Napoca, Cluj-Napoca, Romania
Sechel Niculina A.: Materials Science and Engineering Department, Technical University of Cluj-Napoca, Cluj-Napoca, Romania
Neamțu Bogdan V.: Materials Science and Engineering Department, Technical University of Cluj-Napoca, Cluj-Napoca, Romania
Marinca Traian F.: Materials Science and Engineering Department, Technical University of Cluj-Napoca, Cluj-Napoca, Romania
Popa Florin: Materials Science and Engineering Department, Technical University of Cluj-Napoca, Cluj-Napoca, Romania
Chicinaș Horea F.: Materials Science and Engineering Department, Technical University of Cluj-Napoca, Cluj-Napoca, Romania
Chicinaș Ionel: Materials Science and Engineering Department, Technical University of Cluj-Napoca, Cluj-Napoca, Romania

DOI: https://doi.org/10.2298/SOS2203335P
Journal volume & issue: Vol. 54, no. 3
pp. 335 – 347

Abstract

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Fe-base Superalloy/Al2O3 type composite compacts were successfully obtained by spark plasma sintering from mechanically alloyed powders. The superalloy powders without Al2O3 and superalloy/Al2O3 type composites powders with 5 and 10 %vol. Al2O3 were synthesized from elemental powders in a high energy planetary mill. The influence of the milling process on particle size evolution has been determined using a Laser Particle Size Analyzer with an analysis field of 0.1-1000 μm. The composite compacts were obtained by spark plasma sintering. Both, composite powders, and compacts were investigated by X-ray diffraction (XRD), high temperature X-ray diffraction (HT-XRD), scanning electron microscopy (SEM) and energy dispersive X-ray spectroscopy (EDX).

Published in Science of Sintering

ISSN: 0350-820X (Print); 1820-7413 (Online)
Publisher: International Institute for the Science of Sintering, Beograd
Country of publisher: Serbia
LCC subjects: Technology: Chemical technology
Website: http://www.doiserbia.nb.rs/journal.aspx?issn=0350-820X

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