Sensors (Sep 2022)
Ultrasonic Monitoring of the Water Content in Concentrated Water–Petroleum Emulsions Using the Slope of the Phase Spectrum
Abstract
This work proposes the slope of the phase spectrum as a signal processing parameter for the ultrasonic monitoring of the water content of water-in-crude oil emulsions. Experimental measurements, with water volume fractions from 0 to 0.48 and test temperatures of 20 °C, 25 °C, and 30 °C, were carried out using ultrasonic measurement devices operating in transmission–reception and backscattering modes. The results show the phase slope depends on the water volume fraction and, to a lesser extent, on the size of the emulsion droplets, leading to a stable behavior over time. Conversely, the behavior of the phase slope as a function of the volume fraction is monotonic with low dispersion. Fitting a power function to the experimental data provides calibration curves that can be used to determine the water content with percentage relative error up to 70% for a water volume fraction of 0.06, but less than 10% for water volume fractions greater than 0.06. Furthermore, the methodology works over a wide range of volume fractions.
Keywords