Acta Crystallographica Section E (Aug 2012)

N-(2,4-Difluorophenyl)-5-methyl-1,2-oxazole-4-carboxamide hemihydrate

  • Jian-Guang Yu,
  • Hai-Xi Zhu,
  • Jiang-Kai Qiu,
  • De-Cai Wang,
  • Hong Xu

DOI
https://doi.org/10.1107/S1600536812029431
Journal volume & issue
Vol. 68, no. 8
pp. o2325 – o2325

Abstract

Read online

In the title compound, C11H8F2N2O2·0.5H2O, the dihedral angle between the benzene and isoxazole rings is 8.08 (3)°. In the crystal, the components are linked by O—H...N and N—H...O hydrogen bonds, in which the water molecule acts as both a donor and an acceptor, into a tape with an R44(16) graph-set motif along the a axis. The water molecule is located on a twofold rotation axis. The methyl H atoms were treated as disordered groups over two sites with a refined site-occupancy ratio of 0.48 (6):0.52 (6).