New insights into the stress rupture life enhancement mechanisms of a nickel-based superalloy

Abstract

In this paper, the effects of hot isostatic pressing (HIP) and heat treatment (HT) on the stress rupture properties of nickel-based superalloy K417G were investigated. Scanning electron microscopy (SEM), electron backscatter diffraction (EBSD) and transmission electron microscopy (TEM) were employed to analyze the microstructure, fracture morphology, determination of crack source and dislocation evolution after stress rupture fracture. The results indicate that, HIP specimens demonstrate a 19.5% reduction in stress rupture life compared to as-cast specimens, whereas HIP + HT specimens exhibit a 41% increase in stress rupture life, reaching a value of 63.04 h. The fracture mechanism of the samples under different heat treatment conditions is different. There are a large number of pores in the as-cast specimen, which leads to the initiation and propagation of cracks and eventually result in fracture. The pores in the HIP specimen are almost eliminated. However, the coarsening and uneven distribution of γ′ phase led to the weakening of the hindrance to dislocation movement. Additionally, the increase in elongated carbides at grain boundaries accelerates crack initiation and propagation. Under HIP and HT, the cubic γ′ phase is uniformly precipitated, which effectively hinders the movement of dislocation lines. Granular M23C6 carbides precipitate at grain boundaries, acting as pinning points to retard grain boundary sliding and crack propagation, thus improving the stress rupture life.

Keywords

• Nickel-based superalloy
• K417G
• HIP
• Stress rupture properties
• Fracture mechanism