The article presents research on the metallurgical synthesis of the CuNiSi alloy with a nickel content of 2,2 wt.% and silicon in the range of 0,8 – 1,3 wt.%. Each of the produced materials were subjected to the process of homogenization, solution heat treatment and artificial aging in order to improve the mechanical and electrical properties. Materials were directed to the chemical composition tests, Vickers hardness and electrical conductivity tests and also for microstructural tests with using scanning electron microscopy (SEM).