Green Processing and Synthesis (Dec 2016)

Study of ATO nanoparticles by the solvothermal method for thermal insulated coated glass: a green energy application

  • Anh Trinh Xuan,
  • Tung Duong Thanh,
  • Nhan Do Quy,
  • Hoang Tran Vinh,
  • Trung Do Quang,
  • Thu Le Dieu,
  • Hoang Phan Huy,
  • Cuong Nguyen Duy

DOI
https://doi.org/10.1515/gps-2016-0068
Journal volume & issue
Vol. 5, no. 6
pp. 529 – 535

Abstract

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Antimony-doped tin oxide (ATO) nanoparticles (NPs) (Sb-doped content 3%, 10%, and 15%) were synthesized by the (2 l autoclave, medium-scale) solvothermal method followed by sintering at various temperatures (500°C, 800°C, 900°C and 1000°C) so they would crystallize. The particle size increased from several to tens of nanometers with the increase of sintered temperature from 500°C to 1000°C, sharply from 800°C to 1000 °C; ~30 g of final product was received for each experiment. More interestingly, the crystallinity of the as-synthesized ATO was also increased with the increasing Sb doped content from 3% to 15%. The ATO NPs were coated onto glass substrates and then sintered at 500°C, which effectively prevented transmittance of infrared (IR) wavelengths (>800 nm) with 10% wt Sb-doped content, which is useful for thermal insulated glass coating application.

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