مجلة التربية والعلم (Dec 2013)

Construction of a selective membrane electrode for the determination of procaine hydrochloride by Schiff bases

  • Siham Amin,
  • Faiz Hamid,
  • Obaid Jassim

DOI
https://doi.org/10.33899/edusj.2013.163079
Journal volume & issue
Vol. 26, no. 5
pp. 60 – 73

Abstract

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ABSTRACT This project including synthesis of selective membrane electrode ,consisting of electrically active material produced from Schiff base reaction of (procaine hydrochloride , m-hydroxyl benzeldehyde) with phosphomolybdic acid and dibutyl phthalate as blastilyzer material and used poly phenyl chloride as asupport material , The electrode gave liner response in the range (10-5-10-1 M) with slope 19.3mvdecade r2=0.9973 and LOD =1.72 ×10-7 M, The Optimum concentration of the inner solution was (10-4) M at temperature (25-35 C°)and pH (6-8) .The Life time of the electrode was105 days.

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